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.Identification of nanosecond-timescale internal motionThe presence of nanosecond-timescale motion can be directly identified from a plot of the normalized ratio of R^sub 1^ values measured at two magnetic fields (RT^sup n^^sub 1^) versus NOE (22)
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. Aggregation occurs at the protein concentrations at which phase separation occurs (The observed phase behavior is consistent with literature measurements of both the second virial coefficient (39,40) and the solid-liquid coexistence line (41)
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